| Preface |
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iii | |
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Chapter 1 Introduction to Gas Chromatography |
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1 | (20) |
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History of Chromatography |
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1 | (5) |
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The Basic Gas Chromatography |
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6 | (3) |
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The Principles of a Chromatographic Separation |
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9 | (2) |
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The Progress of a Solute Through a Chromatographic System |
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11 | (7) |
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18 | (3) |
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Chapter 2 The Mechanism of Retention |
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21 | (44) |
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21 | (8) |
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The Thermodynamic Explanation of Retention |
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29 | (4) |
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33 | (19) |
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Parameters that Control the Chromatographically Available Stationary Phase (Vs) |
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52 | (3) |
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The Resolving Power of a GC Column |
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55 | (5) |
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The Effective Plate Number |
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60 | (4) |
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64 | (1) |
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Chapter 3 Peak Dispersion |
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65 | (36) |
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65 | (3) |
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Alternative Forms of Presenting Chromatographic Data |
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68 | (2) |
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70 | (6) |
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Carrier Gas Compressibility: Its Effect on the Interpretation of Chromatographic Data |
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76 | (6) |
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Effect of Mobile Phase Compressibility on the HETP Equation for a Packed GC Column |
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82 | (4) |
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Extensions of the HETP Equation |
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86 | (3) |
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The Golay Equation for Open Tubular Columns |
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89 | (4) |
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93 | (6) |
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99 | (2) |
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Chapter 4 GC Columns and Their Construction |
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101 | (32) |
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103 | (15) |
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Capillary or Open Tubular Columns |
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118 | (7) |
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Porous Layer Open Tubular (PLOT) Columns |
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125 | (3) |
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128 | (3) |
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131 | (2) |
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Chapter 5 Gas Chromatography Instrumentation |
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133 | (38) |
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The Contemporary Gas Chromatograph |
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134 | (1) |
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135 | (13) |
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148 | (10) |
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158 | (6) |
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164 | (1) |
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Column/Detector Connecting Conduits |
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165 | (1) |
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Data Acquisition and Processing |
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166 | (1) |
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Automatic Sample Processing for GC Analysis |
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167 | (3) |
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170 | (1) |
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Chapter 6 Gas Chromatography Detectors |
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171 | (30) |
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Major Detector Specifications |
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171 | (9) |
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The Flame Ionization Detector |
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180 | (4) |
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The Nitrogen Phosphorus Detector (NPD) |
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184 | (2) |
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The Electron Capture Detector |
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186 | (5) |
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The Katherometer Detector |
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191 | (3) |
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194 | (2) |
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The Pulsed Helium Discharge Detector |
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196 | (3) |
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199 | (2) |
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Chapter 7 Sample Preparation |
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201 | (24) |
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202 | (8) |
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210 | (4) |
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214 | (4) |
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Derivatization Techniques |
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218 | (5) |
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223 | (2) |
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Chapter 8 Chromatographic Development |
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225 | (32) |
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228 | (7) |
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235 | (9) |
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244 | (7) |
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Purge and Vent Techniques |
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251 | (4) |
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255 | (2) |
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Chapter 9 Qualitative Analysis |
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257 | (30) |
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The Corrected Retention Volume |
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257 | (1) |
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The Capacity Ratio of a Solute |
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258 | (1) |
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259 | (4) |
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Gas Chromatography/Mass Spectrometry (GC/MS) Systems |
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263 | (2) |
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Ionization Techniques for GC/MS |
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265 | (9) |
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Gas Chromatography/Infrared (GC/IR) Systems |
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274 | (8) |
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Inductively Coupled Plasma (ICP) GC/ES Systems |
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282 | (4) |
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286 | (1) |
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Chapter 10 Quantitative Analysis |
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287 | (38) |
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Data Collection and Data Handling |
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290 | (4) |
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Transmission of the Data to the Computer |
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294 | (3) |
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Data Processing and Reporting |
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297 | (1) |
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The Basic Principles of Data Processing |
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298 | (3) |
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301 | (3) |
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The Quantitative Evaluation of the Chromatogram |
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304 | (1) |
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305 | (5) |
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310 | (3) |
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Quantitative Analytical Methods for GC and LC |
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313 | (5) |
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318 | (5) |
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323 | (2) |
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Chapter 11 Gas Chromatography Applications |
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325 | (66) |
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330 | (7) |
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337 | (8) |
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Food and Beverage Products |
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345 | (8) |
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Biotechnology Applications |
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353 | (13) |
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Environmental Applications |
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366 | (8) |
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374 | (12) |
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General Comments on Analytical Gas Chromatography |
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386 | (2) |
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388 | (3) |
| Index |
|
391 | |
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