9780030340635

Experimental Organic Chemistry A Miniscale and Microscale Approach (with CD-ROM)

by Unknown
  • ISBN13:

    9780030340635

  • ISBN10:

    0030340632

  • Edition: 3rd
  • Format: Hardcover
  • Copyright: 10/9/2001
  • Publisher: Brooks Cole
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Supplemental Materials

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Summary

This proven and well-tested laboratory manual for organic chemistry students contains procedures for both miniscale (also known as small scale) and microscale users. This lab manual gives students all the necessary background to enter the laboratory with the knowledge to perform the experiments with confidence. For the microscale labs, experiments were chosen to provide tangible quantities of material, which can then be analyzed. Chapters 1-2 introduce students to the equipment, record keeping, and safety of the laboratory. Chapters 3-6, and 8 are designed to introduce students to laboratory techniques needed to perform all experiments. In Chapters 7 and 9 through 20, students are required to use the techniques to synthesize compounds and analyze their properties. In Chapter 21, students are introduced to multi-step syntheses of organic compounds, a practice well known in chemical industry. In Chapter 23, students are asked to solve structures of unknown compounds. The new chapter 24 introduces a meaningful experiment into the textbook that reflects the increasing emphasis on bioorganic chemistry in the sophomore-level organic lecture course. This experiment not only gives students the opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide but also provides valuable experience regarding the role of protecting groups in effecting synthetic transformations with multiple functionalized molecules.

Table of Contents

1. Introduction, Record Keeping, and Laboratory Safety
2. Techniques and Apparatus
3. Solids: Recrystallization and Melting Points
4. Liquids
5. Extraction
6. Chromatography
7. Stereoisomers
8. Spectral Methods
9. Alkanes
10. Alkenes
11. Alkynes
12. Dienes: The Diels-Alder Reaction
13. Kinetic and Thermodynamic Control of a Reaction
14. Nucleophilic Aliphatic Substitution: Preparation for Alkyl Halides
15. Electrophilic Aromatic Substitution
16. Oxidation of Alcohols and Carbonyl Compounds
17. Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and Imines
18. Reactions of Carbonyl Compounds
19. Organometallic Chemistry
20. Carboxylic Acids and Their Derivatives
21. Polymers
22. Carbohydrates
23. Identifying Organic Compounds
24. The Literature of Organic Chemistry

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