Fundamentals of Analytical Chemistry

by Skoog, Douglas A.; Holler, F. James

• ISBN13: 9780030059384
• ISBN10: 0030059380
• Format: Hardcover
• Copyright: 1995-08-25
• Publisher: Brooks Cole

Summary

Readability combined with a systematic and rigorous approach characterizes this classic text. Extensive coverage of the principles and practices of quantitative chemistry ensures suitability for chemistry majors.

Table of Contents

Introduction	1	(10)
Errors in Chemical Analyses	11	(10)
Random Errors in Analyses	21	(26)
Application of Statistics to Data Treatment and Evaluation	47	(24)
Gravimetric Methods of Analysis	71	(29)
Titrimetric Methods of Analysis	100	(22)
Aqueous-Solution Chemistry	122	(26)
Effects of Electrolytes on Ionic Equilibria	148	(11)
Application of Equilibrium Calculations to Complex Systems	159	(30)
Theory of Neutralization Titrations	189	(35)
Titration Curves for Complex Acid/Base Systems	224	(24)
Applications of Neutralization Titrations	248	(18)
Precipitation Titrimetry	266	(12)
Complex-Formation Titrations	278	(25)
An Introduction to Electrochemistry	303	(27)
Applications of Standard Electrode Potentials	330	(30)
Applications of Oxidation/Reduction Titrations	360	(26)
Theory of Potentiometry	386	(26)
Applications of Potentiometry	412	(19)
Electrogravimetric and Coulometric Methods	431	(29)
Voltammetry	460	(37)
An Introduction to Spectrochemical Methods	497	(30)
Instruments for Optical Spectrometry	527	(30)
Molecular Absorption Spectroscopy	557	(44)
Molecular Fluorescence Spectroscopy	601	(10)
Atomic Spectroscopy Based on Ultraviolet and Visible Radiation	611	(26)
Kinetic Methods of Analysis	637	(23)
An Introduction to Chromatographic Methods	660	(26)
Gas-Liquid Chromatography	686	(15)
High-Performance Liquid Chromatography	701	(24)
The Analysis of Real Samples	725	(11)
Preparing Samples for Analysis	736	(13)
Decomposing and Dissolving the Sample	749	(11)
Eliminating Interferences	760	(18)
The Chemicals, Apparatus, and Unit Operations of Analytical Chemistry	778	(34)
Selected Methods of Analysis	812
Glossary	G-1
Appendix 1 Selected References to the Literature of Analytical Chemistry	A-1
Appendix 2 Solubility Product Constants	A-6
Appendix 3 Dissociation Constants for Acids	A-8
Appendix 4 Stepwise Formation Constants	A-10
Appendix 5 Some Standard and Formal Electrode Potentials	A-12
Appendix 6 Designations Carried by Ashless Filter Papers	A-16
Appendix 7 Designations and Porosities for Filtering Crucibles	A-17
Appendix 8 Use of Exponential Numbers and Logarithms	A-18
Appendix 9 Volumetric Calculations Using Normality and Equivalent Weight	A-23
Appendix 10 Compounds Recommended for the Preparation of Standard Solutions of Common Elements	A-32
Appendix 11 Propagation of Measurements Uncertainties	A-34
Answers to Selected Questions and Problems	A-40
Index	I-1