Experimental Organic Chemistry : A Miniscale and Microscale Approach

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  • Edition: 5th
  • Format: Hardcover
  • Copyright: 2010-01-19
  • Publisher: Brooks Cole
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This proven laboratory manual for organic chemistry contains procedures for both miniscale (also known as small scale) and microscale users. EXPERIMENTAL ORGANIC CHEMISTRY covers the background and laboratory techniques readers need to perform the book's experiments with confidence. Chapters show readers how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds.

Table of Contents

Introduction, Record Keeping, and Laboratory Safety
Techniques and Apparatus
Solids: Recrystallization and Melting Points
Liquids: Distillation and Boiling Points
Spectral Methods
Dienes: the Diels-Alder Reaction
Kinetic and Thermodynamic Control of a Reaction
Nucleophilic Aliphatic Substitution: Preparation for Alkyl Halides
Electrophilic Aromatic Substitution
Oxidation of Alcohols and Carbonyl Compounds
Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and Imines
Reactions of Carbonyl Compounds
Organometallic Chemistry
Carboxylic Acids and Their Derivatives
Multistep Organic Synthesis
Amino Acids and Peptides
Identifying Organic Compounds
The Literature of Organic Chemistry
Table of Contents provided by Publisher. All Rights Reserved.

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