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| Introduction to Basic Laboratory Techniques | |
| Solubility | |
| Crystallization | |
| Extraction | |
| Chromatography | |
| Simple and Fractional Distillation | |
| Infrared Spectroscopy and Boiling-Point Determination | |
| Essay: Aspirin | |
| Acetylsalicylic Acid | |
| Essay: Analgesics | |
| Acetanilide | |
| Acetaminophen | |
| Essay: Identification of Drugs | |
| TLC Analysis of Analgesic Drugs | |
| Essay: Caffeine | |
| Isolation of Caffeine | |
| Experiment | |
| Isolation of Caffeine from Tea Leaves | |
| Experiment | |
| Isolation of Caffeine from a Tea Bag | |
| Essay: Esters -- Flavors and Fragrances | |
| Isopentyl Acetate (Banana Oil) | |
| Methyl Salicylate (Oil of Wintergreen) | |
| Essay: Terpenes and Phenylpropanoids | |
| Isolation of Eugenol from Cloves | |
| Essay: Stereochemical Theory of Odor | |
| Spearmint and Caraway Oil: (+)- and (-)- Carvones | |
| Essay: The Chemistry of Vision | |
| Isolation of Chlorophyll and Carotenoid Pigments from Spinach | |
| Essay: Ethanol and Fermentation Chemistry | |
| Ethanol from Sucrose | |
| Introduction to Molecular Modeling | |
| Essay: Molecular Modeling and Molecular Mechanics | |
| An Introduction to Molecular Modeling | |
| The Conformations of n-Butane: Local Minima | |
| Cyclohexane Chair and Boat Conformations | |
| Substituted Cyclohexane Rings | |
| cis- and trans-2-Butene | |
| Essay: Computational Chemistry -- Ab initio and Semiempirical Methods | |
| Computational Chemistry | |
| Heats of Formation: Isomerism, Tautomerism, and Regioselectivity | |
| Heats of Reactions: SN1 Reaction Rates | |
| Density-Electrostatic Potential | |
| Maps -- Acidities of Carboxylic Acids | |
| Density -- Electrostatic Potential Maps: Carbocations | |
| Density -- LUMO Maps: Reactivities of Carbonyl Groups | |
| Properties and Reactions of Organic Compounds | |
| Reactivities of Some Alkyl Halides | |
| Nucleophilic Substitution Reactions: Competing Nucleophiles | |
| Competing Nucleophiles with 1-Butanol or 2-Butanol | |
| Competing Nucleophiles with 2-Methyl-2-Propanol | |
| Analysis | |
| Hydrolysis of Some Alkyl Chlorides | |
| Synthesis of n-Butyl Bromide and t-Pentyl Chloride | |
| n-Butyl Bromide | |
| t-Pentyl Chloride | |
| 4-Methylcyclohexene | |
| Phase-Transfer Catalysis: Addition of Dichlorocarbene to Cyclohexene Essay: Fats and Oils | |
| Methyl Stearate from Methyl Oleate | |
| Essay: Soaps and Detergents | |
| Preparation of Soap | |
| Preparation of a Detergent | |
| Essay: Petroleum and Fossil Fuels | |
| Gas Chromatographic Analysis of Gasolines | |
| Essay: Detection of Alcohol: The Breathalyzer | |
| Chromic Acid Oxidation of Alcohols | |
| Chromic Acid Oxidation of Alcohols -- Visible Spectrophotometer Method | |
| Chromic Acid Oxidation of Alcohols -- UV-VIS Spectrophotometer Method | |
| Essay: Green Chemistry | |
| Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination | |
| Chiral Reduction of Ethyl Acetoacetate | |
| NMR Determination of the Optical Purity of (S)-Ethyl 3-Hydroxybutanoate | |
| Nitration of Aromatic Compounds Using a Recyclable Catalyst | |
| An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol | |
| Multi-Step Reaction Sequences: The Conversion of Benzaldehyde to Benzilic Acid | |
| Preparation of Benzoin by Thiamine Catalysis | |
| Preparation of Benzil | |
| Preparation of Benzilic Acid | |
| Tetraphenylcyclopentadienone | |
| Triphenylmethanol and Benzoic Acid | |
| Triphenylmethanol | |
| Benzoic Acid | |
| Resolution of (+/-)-alpha-Phenylethylamine and Determination of Optical Purity | |
| Resolution of (+/-)-alpha-Phenylethylamine | |
| Determination of Optical Purity Using NMR and a Chiral Resolving Agent | |
| The Aldol Condensation Reaction: Preparation of Benzalacetophenones Chalcones) | |
| Preparation of an alpha,beta-Unsaturated Ketone via Michael and Aldol Condensation Reactions | |
| Enamine Reactions: 2-Acetylcyclohexanone | |
| 1,4-Diphenyl-1,3-Butadiene | |
| Relative Reactivities of Several Aromatic Compounds | |
| Nitration of Methyl Benzoate | |
| Essay: Local Anesthetics | |
| Benzocaine | |
| Essay: Pheromones: Insect Attractants and Repellents | |
| N,N-Diethyl-m-Toluamide: The Insect Repellent "OFF" | |
| Essay: Sulfa Drugs | |
| Sulfa Drugs: Preparation of Sulfanilamide | |
| Essay: Food Colors | |
| Chromatography of Some Dye Mixtures | |
| Essay: Polymers and Plastics | |
| Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene | |
| Polyesters | |
| Polyamide (Nylon) | |
| Polystyrene | |
| Infrared Spectra of Polymer Samples | |
| Essay: Diels-Alder Reactions and Insecticides | |
| The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride | |
| Photoreduction of Benzophenone and Rearrangement of Benzpinacol to Benzopinacolone | |
| Photoreduction of Benzophenone | |
| Synthesis of beta-Benzopinacolone: The Acid-Catalyzed Rearrangement of Benzpinacol | |
| Essay: Fireflies and Photochemistry | |
| Luminol | |
| Essay: The Chemistry of Sweeteners | |
| Carbohydrates | |
| Analysis of a Diet Soft Drink by HPLC | |
| Essay: Chemistry of Milk | |
| Isolation of Casein and Lactose from Milk | |
| Isolation of Casein from Milk | |
| Isolation of Lactose from Milk | |
| Identification of Organic Substances | |
| Identification of Unknowns | |
| Solubility Tests | |
| Tests for the Elements (N, S, X) | |
| Tests for Unsaturation | |
| Aldehydes and Ketones | |
| Carboxylic Acids | |
| Phenols | |
| Amines | |
| Alcohols | |
| Esters | |
| Project-Based Experiments | |
| Preparation of a C-4 or C-5 Acetate Ester | |
| A Separation and Purification Scheme | |
| Extractions with a separatory funnel | |
| Extractions with a Screw-Cap centrifuge tube | |
| Isolation of Essential Oils from Allspice, Cloves, Cumin, Caraway, Cinnamon, or Fennel | |
| Isolation of Essential Oils by Steam Distillation | |
| Identification of the Constituents of Essential Oils by Gas Chromatography-Mass Spectrometry | |
| Investigation of the Essential Oils of Herbs and Spices-Mini-Research Project | |
| Friedel-Crafts Acylation | |
| The Analysis of Antihistamine Drugs by Gas Chromatography-Mass Spectrometry | |
| Carbonation of an Unknown Aromatic Halide | |
| The Aldehyde Enigma | |
| Synthesis of Substituted Chalcones: A Guided-Inquiry Experience | |
| Michael and Aldol Condensation Reactions | |
| Esterification Reactions of Vanillin: The Use of NMR to Solve a Structure Proof Problem | |
| An Oxidation Puzzle | |
| The Techniques | |
| Laboratory Safety | |
| The Laboratory Notebook, Calculations, and Laboratory Records | |
| Laboratory Glassware: Care and Cleaning | |
| How to Find Data for Compounds: Handbooks and Catalogues | |
| Measurement of Volume and Weight | |
| Heating and Cooling Methods | |
| Reaction Methods | |
| Filtration | |
| Physical Constants of Solids: The Melting Point | |
| Solubility | |
| Crystallization: Purification of Solids | |
| Extractions, Separations, and Drying Agents | |
| Physical Constants of Liquids: The Boiling Point and Density | |
| Simple Distillation | |
| Fractional Distillation, Azeotropes | |
| Vacuum Distillation, Manometers | |
| Sublimation | |
| Steam Distillation | |
| Column Chromatography | |
| Thin-Layer Chromatography | |
| High-Performance Liquid Chromatography (HPLC) | |
| Gas Chromatography | |
| Polarimetry | |
| Refractometry | |
| Infrared Spectroscopy | |
| Nuclear Magnetic Resonance Spectroscopy (Proton NMR) | |
| Carbon-13 Nuclear Magnetic Resonance Spectroscopy | |
| Mass Spectrometry | |
| Guide to the Chemical Literature | |
| Tables of Unknowns and Derivatives | |
| Procedure for Preparing Derivatives | |
| Index of Spectra. | |
| Table of Contents provided by Publisher. All Rights Reserved. |
The New copy of this book will include any supplemental materials advertised. Please check the title of the book to determine if it should include any access cards, study guides, lab manuals, CDs, etc.
The Used, Rental and eBook copies of this book are not guaranteed to include any supplemental materials. Typically, only the book itself is included. This is true even if the title states it includes any access cards, study guides, lab manuals, CDs, etc.
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