9780030343117

Microscale and Macroscale Techniques in the Organic Laboratory

by ; ; ;
  • ISBN13:

    9780030343117

  • ISBN10:

    0030343119

  • Format: Hardcover
  • Copyright: 2001-08-13
  • Publisher: Cengage Learning

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Supplemental Materials

What is included with this book?

Summary

The well-known and tested organic chemistry laboratory techniques of the two best-selling organic chemistry lab manuals: INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A SMALL SCALE APPROACH and INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A MICROSCALE APPROACH, 3/e are now assembled in one textbook. Professors can use any experiments alongside MICROSCALE AND MACROSCALE TECHNIQUES IN THE ORGANIC LABORATORY. Experiments can be selected and assembled from the two Pavia organic chemistry lab manuals, from professors' homegrown labs, or even competing texts. The 375 page, hardcover book serves as a reference for all students of organic chemistry. With clearly written prose and accurately drawn diagrams, students can feel confident setting up and running organic labs.

Table of Contents

1. Laboratory Safety
2. Advance Preparation and Laboratory Records
3. Laboratory Glassware
4. How to Find Data for Your Compound: Handbooks and Catalogues
5. Measurement of Volume and Weight
6. Heating and Cooling Methods
7. Reaction Methods
8. Filtration
9. Physical Constants of Solids: The Melting Point
10. Solubility
11. Crystallization: Purification of Solids
12. Extractions, Separations, and Drying Agents
13. Physical Constants of Liquids: Boiling Point and Density
14. Simple Distillation
15. Fractional Distillation; Azeotropes
16. Vacuum Distillation; Manometers
17. Sublimation
18. Steam Distillation
19. Column Chromatography
20. Thin-Layer Chromatography
21. High-Performance Liquid Chromatography (HPLC)
22. Gas Chromatography
23. Polarimetry
24. Refractometry
25. Infrared Spectroscopy
26. Nuclear Magnetic Resonance Spectroscopy (Proton NMR)
27. Carbon-13 Nuclear Magnetic Resonance Spectroscopy
28. Mass Spectrometry
29. Computational Chemistry
30. Guide to the Chemical Literature

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