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9780892364695

Infrared Spectroscopy in Conservation Science

by ; ;
  • ISBN13:

    9780892364695

  • ISBN10:

    0892364696

  • Edition: 1st
  • Format: Paperback
  • Copyright: 2000-03-16
  • Publisher: J Paul Getty Museum Pubns
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List Price: $75.00

Summary

These volumes provide useful scientific procedures and methodologies for the practice of conservation.Provides techniques for examining the microscopic amounts of complex, aged components in objects such as paintings, sculptures, and archaeological fragments.

Table of Contents

Foreword vii
Preface ix
Acknowledgments xi
History of Infrared Spectroscopy
1(3)
Additional Reading
3(1)
Infrared Absorption Theory
4(12)
Electromagnetic Radiation
4(2)
Wave Theory
4(2)
Absorption Theory
6(6)
Molecular Absorptions
8(1)
Degrees of Freedom
8(3)
Selection Rules
11(1)
Group Frequencies
11(1)
Infrared Spectra
12(1)
Infrared Regions
13(1)
Near-Infrared Region
13(1)
Mid-Infrared Region
13(1)
Far-Infrared Region
14(1)
Summary
14(1)
Additional Reading
15(1)
Sample Collection and Preparation
16(27)
Sampling Methodology
16(4)
Sampling Design
17(2)
Sampling Location
19(1)
Sampling Implementation
20(4)
Tools
20(1)
Sample Documentation and Storage
21(2)
Avoidance of Contamination
23(1)
Sample Collection and Preparation Procedures
24(18)
Gases
24(1)
Liquids
25(1)
Sampling with Swabs
26(2)
Solids, Powders, and Particles
28(4)
Fibers
32(1)
Cross Sections
33(9)
Summary
42(1)
Additional Reading
42(1)
Infrared Analysis Methods
43(39)
Infrared Transmission Measurements
45(15)
Infrared Window Materials
46(4)
Transmission Analysis of Gases
50(1)
Transmission Analysis of Liquids
50(2)
Transmission Analysis of Solids
52(8)
Infrared Reflection Measurements
60(8)
Specular Reflection
62(1)
Reflection-Absorption
63(1)
Diffuse Reflection
63(2)
Internal Reflection
65(3)
Infrared Microspectroscopy
68(12)
Microspectrophotometer Design
69(1)
Microspectrophotometer Capabilities
69(1)
Particle and Fiber Analysis
70(6)
Cross Section Analysis
76(3)
Microspectrophotometer Accessories
79(1)
Summary
80(1)
Additional Reading
80(2)
Spectral Interpretation
82(48)
Infrared Spectra
82(5)
Absorption Bands
82(2)
Plotting Format
84(2)
Instrument Configuration
86(1)
Qualitative Analysis
87(13)
Spectral Quality
87(4)
Visual Comparison
91(1)
Computer Libraries
92(1)
Spectral Region Examination
93(2)
Spectra-Structure Correlations
95(4)
Correlation Charts
99(1)
Identification of Materials Used in Art and Art Conservation
100(21)
Natural Organic Materials
100(9)
Synthetic Resins (Polymers)
109(4)
Colorants
113(7)
Mixtures
120(1)
Quantitative Analysis
121(3)
Mathematical Manipulations of Spectra
124(3)
Subtraction Techniques
124(1)
Resolution Enhancement Methods
125(2)
Summary
127(2)
Additional Reading
129(1)
Case Studies 130(42)
Identification and Characterization of Materials
130(3)
Deterioration Studies
133(1)
The Case Studies
134(37)
Case Study 1: Ultramarine Pigments
134(4)
Case Study 2: Creosote Lac Resin
138(3)
Case Study 3: Chumash Indian Paints
141(3)
Case Study 4: Varnish on a Desk
144(4)
Case Study 5: Reflection versus Transmission
148(4)
Case Study 6: Painting Cross Sections
152(3)
Case Study 7: Vikane
155(4)
Case Study 8: Parylene
159(4)
Case Study 9: Cellulose Nitrate Sculptures
163(3)
Case Study 10: Dead Sea Scrolls
166(5)
Summary
171(1)
Appendix I: Selected Infrared Spectra Collections and Digitized Libraries 172(6)
Appendix II: Infrared Reference Spectra 178(23)
Glossary 201(4)
Suppliers 205(2)
References 207(23)
Index 230(6)
About the Authors 236

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