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Introduction to Principles and Practice of Mass Spectrometry | p. 1 |
History of Mass Spectrometry | p. 1 |
Ionisation of Molecules | p. 3 |
Ion Separation | p. 18 |
Ion Detection | p. 22 |
Metastable Ions, Collision Induced Dissociation and Tandem Mass Spectrometry | p. 23 |
Scanning Modes | p. 29 |
References | p. 32 |
Interpretation of Organic Mass Spectrometric Data | p. 33 |
Introduction | p. 33 |
Formation of the Electron Ionisation Mass Spectrum | p. 34 |
Calibration of the Mass Scale and Determination of Molecular Mass | p. 37 |
Interpretation of High- and Low-resolution Data | p. 39 |
An Empirical Approach to the Elucidation of Organic Structures | p. 40 |
Additional Information from the Mass Spectrum | p. 44 |
Classical Fragmentation Processes Occurring in EIMS | p. 46 |
Some Useful Examples of Features of the Mass Spectrum by Chemical Class | p. 52 |
References | p. 54 |
Food Flavourings and Taints | p. 55 |
Introduction | p. 55 |
Flavour Analyses | p. 63 |
Taints and Off-flavours | p. 76 |
Flavour Chemistry | p. 77 |
Aroma Release From Foods | p. 81 |
Breath and Body Odours | p. 85 |
Authentication of Natural and Synthetic Food Components | p. 85 |
Data Processing and Statistical Analysis | p. 86 |
References | p. 87 |
Bioactive Non-nutrients in Foods | p. 93 |
Introduction | p. 93 |
Alkaloids | p. 94 |
Coumarins | p. 105 |
Cyanogenic Compounds | p. 107 |
Glucosinolates | p. 109 |
Mutagenic Heterocyclic Amines Generated by Cooking | p. 114 |
Mycotoxins | p. 117 |
Phytoalexins | p. 134 |
Phenolic Compounds | p. 134 |
Saponins | p. 153 |
References | p. 157 |
Amino Acids, Peptides and Proteins | p. 170 |
Introduction | p. 170 |
Chemical and Enzymatic Studies | p. 174 |
Applications of Mass Spectrometry to Amino Acid, Peptide and Protein Analysis in Food, Nutrition and Agricultural Research | p. 175 |
The Amino Acid Sequencing of Peptides and Proteins | p. 179 |
References | p. 187 |
Lipids | p. 192 |
Introduction | p. 192 |
Derived Lipids | p. 193 |
Simple Lipids | p. 196 |
Compounds Lipids | p. 203 |
Lipid Oxidation Products | p. 208 |
References | p. 210 |
Sugars and Carbohydrates | p. 213 |
Introduction | p. 213 |
Analysis of Sugar Residues: GC/MS of Derivatised Sugars | p. 215 |
Partially Methylated Alditol Acetate (PMAA) Analysis of Linkage and Sugar Type | p. 216 |
Recent Methods for the Determination of Molecular Size | p. 217 |
The Separation of Oligosaccharides by LC/MS | p. 220 |
Sequence Determination of Oligosaccharides | p. 220 |
References | p. 223 |
Quantification and Metabolism of Inorganic Nutrients | p. 225 |
Introduction | p. 225 |
Sample Collection and Treatment for Inorganic Mass Spectrometry | p. 226 |
Quantitative Applications of TIMS | p. 227 |
Quantitative Applications of ICP-MS | p. 228 |
Metabolic Studies of Inorganic Nutrients | p. 228 |
Sample Preparation for Inorganic Mass Spectrometry | p. 230 |
Mass Spectrometric Techniques for Inorganic Nutrient Studies | p. 231 |
References | p. 242 |
Analysis and Metabolism of Vitamins in Foods | p. 244 |
Introduction | p. 244 |
Water-soluble Vitamins | p. 245 |
Fat-soluble Vitamins | p. 258 |
General Conclusions and Recommendations | p. 268 |
References | p. 268 |
Stable Isotope Studies of Organic Macronutrient Metabolism | p. 273 |
Introduction | p. 273 |
Mass Spectrometric Techniques Used in Macronutrient Metabolism Studies | p. 273 |
Protein Metabolism | p. 273 |
Carbohydrate Metabolism | p. 275 |
Lipid Metabolism | p. 278 |
Whole Body Energy Expenditure | p. 279 |
General Conclusions and Recommended Methods | p. 280 |
References | p. 281 |
Pyrolysis Mass Spectrometry of Foods | p. 283 |
Introduction | p. 283 |
Practical Aspects of Py/MS | p. 284 |
Mass Spectrometric Techniques for Analytical Pyrolysis | p. 284 |
Analysis of Data | p. 285 |
Selected Applications of Py/MS in Food Studies | p. 285 |
Conclusions | p. 288 |
References | p. 290 |
Subject Index | p. 291 |
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The Used, Rental and eBook copies of this book are not guaranteed to include any supplemental materials. Typically, only the book itself is included. This is true even if the title states it includes any access cards, study guides, lab manuals, CDs, etc.