IMPORTANT COVID-19 UPDATES

9783527288267

Spectra Interpretation of Organic Compounds

by ;
  • ISBN13:

    9783527288267

  • ISBN10:

    3527288260

  • Format: Hardcover
  • Copyright: 1997-03-01
  • Publisher: Vch Verlagsgesellschaft Mbh

Note: Supplemental materials are not guaranteed with Rental or Used book purchases.

Purchase Benefits

  • Free Shipping On Orders Over $35!
    Your order must be $35 or more to qualify for free economy shipping. Bulk sales, PO's, Marketplace items, eBooks and apparel do not qualify for this offer.
  • Get Rewarded for Ordering Your Textbooks! Enroll Now
List Price: $135.00 Save up to $33.75
  • Rent Book $121.50
    Add to Cart Free Shipping

    TERM
    PRICE
    DUE
    USUALLY SHIPS IN 3-5 BUSINESS DAYS
    *This item is part of an exclusive publisher rental program and requires an additional convenience fee. This fee will be reflected in the shopping cart.

Supplemental Materials

What is included with this book?

Summary

A unique advanced textbook on spectroscopy. This interactive tutorial presents text, software and data in a state-of-the-art introduction to the interpretation of 13C- and 1H-nuclear magnetic resonance, infrared, mass and UV/VIS spectra. Designed as a hands-on guide, the newcomer or student learns not only by reading but by experimenting, using the powerful software tools and data provided on the accompanying CD-ROM. The software, based on the outstanding SpecTool product, enables you to learn how to interpret molecular spectra correctly, rapidly and easily. Moreover, you can check your progress by working through the examples embedded in this self-study course that demonstrate how to identify an organic compound and to elucidate its structure. All the material and software presented are the essence of the two authors? longstanding teaching experience.

Table of Contents

1 Problem 1
1(8)
1.1 Elemental Composition and Structural Features
4(2)
1.2 Structural Assembly
6(1)
1.3 Comments
6(3)
1.3.1 Mass Spectrum
6(1)
1.3.2 Infrared Spectrum
7(1)
1.3.3 Proton NMR Spectrum
7(1)
1.3.4 Carbon-13 NMR Spectrum
8(1)
2 Problem 2
9(8)
2.1 Elemental Composition and Structural Features
12(1)
2.2 Structural Assembly
13(1)
2.3 Comments
13(4)
2.3.1 Mass Spectrum
13(1)
2.3.2 Infrared Spectrum
14(1)
2.3.3 Proton NMR Spectrum
15(2)
3 Problem 3
17(6)
3.1 Elemental Composition and Structural Features
20(1)
3.2 Structural Assembly
21(1)
3.3 Comments
21(2)
3.3.1 Mass Spectrum
21(1)
3.3.2 Infrared Spectrum
21(1)
3.3.3 Proton and Carbon-13 NMR Spectra
21(2)
4 Problem 4
23(10)
4.1 Elemental Composition and Structural Features
27(1)
4.2 Structural Assembly
27(1)
4.3 Comments
28(5)
4.3.1 Mass Spectrum
28(1)
4.3.2 Infrared Spectrum
28(2)
4.3.3 Proton NMR Spectrum
30(1)
4.3.4 Carbon-13 NMR Spectrum
31(2)
5 Problem 5
33(8)
5.1 Elemental Composition and Structural Features
37(1)
5.2 Structural Assembly
38(1)
5.3 Comments
39(2)
5.3.1 Mass Spectrum
39(1)
5.3.2 Infrared Spectrum
39(1)
5.3.3 Proton NMR Spectrum
39(1)
5.3.4 Carbon-13 NMR Spectrum
40(1)
6 Problem 6
41(10)
6.1 Elemental Composition and Structural Features
45(1)
6.2 Structural Assembly
46(1)
6.3 Comments
46(5)
6.3.1 Mass Spectrum
46(1)
6.3.2 Infrared Spectrum
47(1)
6.3.3 Proton NMR Spectrum
47(2)
6.3.4 Ultraviolet Spectrum
49(2)
7 Problem 7
51(8)
7.1 Elemental Composition and Structural Features
54(1)
7.2 Structural Assembly
55(1)
7.3 Comments
56(3)
7.3.1 Mass Spectrum
56(1)
7.3.2 Infrared Spectrum
56(1)
7.3.3 Proton NMR Spectrum
56(1)
7.3.4 Carbon-13 NMR Spectrum
57(2)
8 Problem 8
59(8)
8.1 Elemental Composition and Structural Features
62(1)
8.2 Structural Assembly
63(1)
8.3 Comments
64(2)
8.3.1 General
64(1)
8.3.2 Mass Spectrum
64(1)
8.3.3 Infrared Spectrum
65(1)
8.3.4 Proton NMR Spectrum
65(1)
8.3.5 Carbon-13 NMR Spectrum
66(1)
8.4 References
66(1)
9 Problem 9
67(10)
9.1 Elemental Composition and Structural Features
71(1)
9.2 Structural Assembly
72(1)
9.3 Comments
73(2)
9.3.1 Mass Spectrum
73(1)
9.3.2 Infrared Spectrum
74(1)
9.3.3 Proton and Carbon-13 NMR Spectra
74(1)
9.4 References
75(2)
10 Problem 10
77(8)
10.1 Elemental Composition and Structural Features
80(1)
10.2 Structural Assembly
81(1)
10.3 Comments
82(3)
10.3.1 Mass Spectrum
82(1)
10.3.2 Infrared Spectrum
83(1)
10.3.3 Ultraviolet Spectrum
83(2)
11 Problem 11
85(8)
11.1 Elemental Composition and Structural Features
88(2)
11.2 Structural Assembly
90(1)
11.3 Comments
91(1)
11.3.1 Mass Spectrum
91(1)
11.3.2 Proton and Carbon-13 NMR Spectra
91(1)
11.4 References
91(2)
12 Problem 12
93(8)
12.1 Elemental Composition and Structural Features
97(1)
12.2 Structural Assembly
98(1)
12.3 Comments
98(3)
12.3.1 Mass Spectrum
98(1)
12.3.2 Infrared Spectrum
99(1)
12.3.3 Proton NMR Spectrum
99(1)
12.3.4 Carbon-13 NMR Spectrum
100(1)
13 Problem 13
101(12)
13.1 Elemental Composition and Structural Features
107(1)
13.2 Structural Assembly
108(1)
13.3 Comments
108(5)
13.3.1 Mass Spectrum
108(2)
13.3.2 Proton and Carbon-13 NMR Spectra
110(1)
13.3.3 Infrared Spectrum
111(2)
14 Problem 14
113(10)
14.1 Elemental Composition and Structural Features
117(1)
14.2 Structural Assembly
118(1)
14.3 Comments
119(4)
14.3.1 Mass Spectrum
119(1)
14.3.2 Infrared Spectrum
120(1)
14.3.3 Proton NMR Spectrum
120(3)
15 Problem 15
123(10)
15.1 Elemental Composition and Structural Features
128(1)
15.2 Structural Assembly
129(1)
15.3 Comments
130(1)
15.3.1 Mass Spectrum
130(1)
15.3.2 Infrared Spectrum
131(1)
15.3.3 Proton NMR Spectrum
131(1)
15.4 References
131(2)
16 SpecTool
133(4)
16.1 What is SpecTool?
133(1)
16.2 What is Hypermedia
133(1)
16.3 Contents of SpecTool
134(1)
16.4 Basic Organization Units
134(1)
16.5 Links
135(1)
16.6 Limitations of the Current Implementation and Known Problems
135(2)
17 Mass Spectrometry: Additional Remarks
137(6)
17.1 Presentation of Data
137(1)
17.2 Degree of Unsaturation. Calculation of Number of Double Bond Equivalents
137(1)
17.3 General Information from Mass Spectra
138(1)
17.4 Evidence for Elemental Composition from Isotope Peak Intensities
139(1)
17.5 Evidence for Elemental Composition in Low Resolution Mass Spectra
140(1)
17.6 High Resolution Data
141(1)
17.7 Impurities in Mass Spectra
141(2)
18 Infrared Spectroscopy: Additional Remarks
143(4)
18.1 Presentation of Data
143(1)
18.2 Prediction of Infrared Stretching Frequencies
143(1)
18.3 Overtones, Combination Bands, Fermi Resonance
144(1)
18.4 Band Shapes and Intensities in Infrared Spectra
145(1)
18.5 Spurious Bands in Infrared Spectra
146(1)
19 NMR Spectroscopy: Additional Remarks
147(14)
19.1 Presentation of Spectra
147(1)
19.1.1 Proton NMR Spectra
147(1)
19.1.2 Carbon-13 NMR Spectra
147(1)
19.2 Rules for the Interpretation of Coupling Patterns
147(5)
19.2.1 Definitions
147(1)
19.2.2 General Rules
148(1)
19.2.3 First order Spectra
149(2)
19.2.4 Higher Order Spectra
151(1)
19.2.5 Computer Simulation
151(1)
19.3 Signal Intensities in Carbon-13 NMR Spectra
152(2)
19.3.1 Saturation
152(1)
19.3.2 Nuclear Overhauser Effect
153(1)
19.3.3 Intensities of Solvent Signals
154(1)
19.4 Influence of Molecular Symmetry and Conformational Equilibria on NMR Spectra
154(5)
19.4.1 Introduction
154(1)
19.4.2 Definitions
154(1)
19.4.3 Influence of Symmetry Properties on the NMR Spectra
155(1)
19.4.4 Influence of Fast Equilibria
155(3)
19.4.5 Examples
158(1)
19.5 References
159(2)
20 Short Introduction to Chem Window
161(8)
20.1 Introduction
161(1)
20.2 Tools
162(5)
20.3 References
167(2)
21 Structures of Compounds
169(4)
Index 173

Rewards Program

Write a Review