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9783527314256

Micro Instrumentation For High Throughput Experimentation and Process Intensification - a Tool for PAT

by ; ;
  • ISBN13:

    9783527314256

  • ISBN10:

    3527314253

  • Format: Hardcover
  • Copyright: 2007-04-09
  • Publisher: Vch Verlagsgesellschaft Mbh
  • Purchase Benefits
List Price: $245.00
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Summary

This first comprehensive treatment of the intertwined roles of micro-instrumentation, high throughput experimentation and process intensification as valuable tools for process analytical technology covers both industrial as well as academic aspects. First class editors and authors from top companies and universities provide interdisciplinary coverage ranging from chemistry and analytics to process design and engineering, supported throughout by case studies and ample analytical data.

Author Biography

Dr. Melvin V. Koch is director of the Center for Process Analytical Chemistry (CPAC) and Affiliate Professor of Chemical Engineering, at the University of Washington in Seattle. He previously worked for the Dow Chemical Company in process research and analytical chemistry, achieving the level of Global Director of Analytical Sciences. Dr. Koch is active in coordinating developments in the field of process analytical technology between industry, government laboratories, and academia. He is serving on the US FDA Advisory Committee for Pharmaceutical Sciences and on review committees at several US National Laboratories.

Dr Kurt M.VandenBussche currently manages the technical resources of UOP's Innovation Group. He holds a Masters and Ph.D. degree in Chemical Engineering from the University of Ghent, Belgium. In 1994, he joined Shell Research and Development in Amsterdam, the Netherlands, as a hydrocracking process specialist. Since joining UOP LLC in December 1996, he has played a number of roles as a reaction engineering and process design consultant and later as technical manager. In 2002, he became a founding member of UOP's Innovation Group. Dr. VandenBussche is member of the executive board of ISCRE Inc and the author of a large number of scientific papers. He is a co-inventor on 15 patents and received the International DSM award for Science and Technology for his contributions in the development of forced unsteady state operation of chemical reactors.

Dr. Ray W. Chrisman is president of Atodyne Technologies and a Visiting Scholar at CPAC. He previously worked for the Dow Chemical Company in various technical and administrative roles in corporate R&D and analytical chemistry. This work involved new technology development and the introduction and use of high throughput technology including the development of patented micro-reactor systems for process characterization. He received a Ph.D. from Purdue University and has published 13 papers and a book chapter in the "Treatise on Analytical Chemistry". He is also the co-inventor on 7 patents.

Table of Contents

Preface.List of Contributors
Introducing the Concepts
Introduction (Melvin V. Koch)
Background
Analytical Tools for use in PAT
The Center for Process Analytical Chemistry (CPAC) and the Summer Institute
Topics covered by Previous CPAC Summer Institutes
Recent Emphasis of CPAC Summer Institutes: High Throughput Experimentation and Process Intensification
Conclusion
Macro to Micro ... The Evolution of Process Analytical Systems
Introduction
Chromatography
Process Intensification
Introduction, Scope and Definitions
Process Intensification in the Field of Reaction Engineering
Process Intensification through Micro-structured Unit Operations
Case Studies
Conclusions
High Throughput Research
Introduction
Description of Terms
Concept of a Research Process
High Throughput Analytical
Extracting Information from the Process
Process Development becomes the Next Bottleneck
Use of High Throughput Concepts for Process Development
Microreactors for Process Development
Current Barriers and Limitations to Microscale Reaction Characterization
Conclusion
Technology Developments and Case Studies
Introduction
Microreactor Concepts and Processing
Introduction
Microreactor Technology - Interfacing and Discipline Cross-boundary Research
Microstructured Mixer-reactors for Pilot and Production Range and Scale-out Issues
Fine-chemical Microreactor Plants
Industrial Microreactor Process Development for Fine and Functional Chemistry
Industrial Production in Fine Chemistry
Microreactor Laboratory-scale Process Developments for Future Industrial Use
Free-radical Polymerizations (Uni Strasbourg, IMM)
Future Directions - Establishing a Novel Chemistry by Enabling Function
Summary
Non-reactor Micro-component Development
Overview
Introduction
Heat Exchange
Mixing
Microchannel Emulsification
Phase Separation
Phase Transfer Processes
Biological Processes
Body Force Driven Processes
Summary and Future Directions
Microcomponent Flow Characterization
Introduction
Pressure Drop
Dimensionless Mechanical Energy Balance
Entry Lengths
Diffusion
Conclusion.N
Table of Contents provided by Publisher. All Rights Reserved.

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