9780125054522

Annual Reports on NMR Spectroscopy: Advances in Solid State NMR Studies of Materials and Polymers

by ; ; ; ; ; ;
  • ISBN13:

    9780125054522

  • ISBN10:

    0125054521

  • Format: Hardcover
  • Copyright: 2004-07-26
  • Publisher: Elsevier Science Serials
  • Purchase Benefits
List Price: $270.00

Summary

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicians to study the structure and dynamics of molecules. In recent years, no other technique has grown to such importance as NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR has established itself as a premier means for the specialist and nonspecialist alike to become familiar with new techniques and applications of NMR spectroscopy.

Table of Contents

List of Contributors v
Preface vii
PISEMA Solid-State NMR Spectroscopy
A. RAMAMOORTHY, YUFENG WEI and DONG-KUK LEE
1. Introduction
2(4)
2. Pulse Sequence
6(8)
3. Experimental Procedure to Optimize the Performance of PISEMA
14(4)
4. Applications of PISEMA
18(27)
5. Proton-Detected PISEMA
45(3)
6. Concluding Remarks
48(1)
Acknowledgements
49(1)
References
50(4)
3D Structure Elucidation Using NMR Chemical Shifts
ULRICH STERNBERG, RAIKER WITTER and ANNE S. ULRICH
1. Introduction
54(2)
2. Basic Concepts of Nuclear Shieldings and Chemical Shifts
56(4)
3. Computational Methods for Chemical Shift Calculations
60(4)
4. Empirical and Semi-Empirical Structure Dependences of Chemical Shifts
64(8)
5. Chemical Shift Derivatives
72(3)
6. Structure Refinement Methods
75(14)
7. Applications in Peptide and Protein Structure Investigations
89(6)
8. Applications in Crystal Structure Refinement
95(3)
References
98(7)
77Se NMR Spectroscopy and Its Applications in Chemistry
HELMUT DUDDECK
1. Introduction
105(1)
2. 77NMR Parameters
106(39)
3. Chemical Applications
145(10)
References
155(12)
Structural Studies of Polymer Blends by Solid-State NMR
HIROMICHI KUROSU and QUN CHEN
1. Introduction
167(1)
2. Miscibility
168(31)
References
199(3)
Structural Characterization of Si-based Polymer Materials by Solid-State NMR Spectroscopy
SHIGEKI KUROKI, HIDEAKI KIMURA and ISAO ANDO
1. Introduction
202(1)
2. Experimental
202(7)
3. Structural Characterization of Si-Based Silyleneethynylene Polymers and Silylenemethylene Polymers Materials
209(11)
4. Structural Characterization of Silicon-Based Interpenetrating Polymer Network Materials
220(12)
5. Structural Characterization of Silyl-Carborane Hybrid Si-Based Polymer Network Materials
232(10)
6. Conclusions
242(1)
References
242(3)
Index 245

Supplemental Materials

What is included with this book?

The New copy of this book will include any supplemental materials advertised. Please check the title of the book to determine if it should include any access cards, study guides, lab manuals, CDs, etc.

The Used, Rental and eBook copies of this book are not guaranteed to include any supplemental materials. Typically, only the book itself is included. This is true even if the title states it includes any access cards, study guides, lab manuals, CDs, etc.

Rewards Program