Basic One- and Two-Dimensional NMR Spectroscopy

by Friebolin, Horst

• ISBN13: 9783527327829
• ISBN10: 3527327827
• Edition: 5th
• Format: Paperback
• Copyright: 2010-12-28
• Publisher: Wiley-VCH

Summary

This is the fifth edition of the highly successful, classic textbook for bachelor and master courses, with over 20 % new material and the contents completely revised and updated. Using a minimum of mathematics, it explains the underlying theory of this most important spectroscopic technique in a thorough, yet readily understandable way, covering instrumentation and interpretation of the spectra. It presents all students need to know about 1D, 2D-NMR, solid state and dynamic NMR spectroscopy, as well as NMR imaging, all illustrated by examples for maximum clarity. All the sections include sub-chapters that focus on applications taken from organic, macromolecular, polymer and biochemistry. A must for students and lecturers in chemistry, biochemistry, pharmacy, and life sciences, as well as for spectroscopists.

Author Biography

Horst Friebolin did his Ph.D. under the supervison of Prof. R. Mecke at the University of Freiburg, Germany, in 1963. Between 1963 and 1979 he worked at the Institute for electronic materials at the Fraunhofer Society and at the Institute for Macromolecular Chemistry at the University of Heidelberg. After two years in industry (BASF, Ludwigshafen, Germany) he finished 1971 his habilitation and joined in 1972 the Institute for Organic Chemistry at the University of Heidelberg, where he was appointed full Professor in 1974. His research fields are the isolation and characterization of natural products as well as enzyme-catalyzed reactions.

Table of Contents

The Physical Basis of NMR Spectroscopy

The Chemical Shift

Indirect Spin-Spin Coupling

Spectrum Analysis and Calculations

Double Resonance Experiments

Assignment of 1H and 13C Signals

Relaxation

One-Dimensional NMR Experiments using Complex Pulse Sequences

Two-Dimensional NMR Spectroscopy

The Nuclear Overhauser Effect

Dynamic NMR Spectroscopy (DNMR)

Shift Reagents

Macromolecules

NMR Spectroscopy in Biochemistry and Medicine

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