Current Developments in Solid State Nmr Spectroscopy

by Muller, Norbert; Madhu, Perunthiruthy K.; Madhu, Perunthiruthy K.

• ISBN13: 9783211838945
• ISBN10: 3211838945
• Format: Hardcover
• Copyright: 2003-05-01
• Publisher: Palgrave-Macmillan

Summary

This book presents some of the latest developments in solid state NMR with potential applications in both materials and biological science. The main emphasis is on a strong link between theory and experiment via numerical simulation of NMR spectra which play a pivotal role in the design and development of pulse schemes in solid state NMR. The papers focus on non-biological topics of solid state NMR spectroscopy making the book useful for scientists and advanced students in chemistry, physics, and materials science striving for deeper understanding of this topic and its application potential. Three invited reviews focus on developments in solid state NMR of quadrupolar nuclei, which are of high interest in areas like materials science and heterogeneous catalysis.

Table of Contents

Invited Reviews
Dipolar and Scalar Couplings in Solid State NMR of Quadrupolar Nuclei	p. 1
Multiple-Quantum Magic-Angle Spinning: High-Resolution Solid State NMR Spectroscopy of Half-Integer Quadrupolar Nuclei	p. 17
Cross-Polarisation Applied to the Study of Liquid Crystalline Ordering	p. 55
Contributions
Improved Proton Decoupling in NMR Spectroscopy of Crystalline Solids Using the Spinal-64 Sequence	p. 69
The Flexibility of SIMPSON and SIMMOL for Numerical Simulations in Solid- and Liquid-State NMR Spectroscopy	p. 75
Residual Dipolar Couplings in [superscript 31]P MAS Spectra of PPh[subscript 3] Substituted Cobalt Complexes	p. 95
Potential and Limitations of 2D [superscript 1]H-[superscript 1]H Spin-Exchange CRAMPS Experiments to Characterize Structures of Organic Solids	p. 107
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