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9780470530184

Chemometric Methods in Capillary Electrophoresis

by ;
  • ISBN13:

    9780470530184

  • ISBN10:

    0470530189

  • Format: eBook
  • Copyright: 2009-10-01
  • Publisher: Wiley
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Summary

Use chemometric techniques to develop optimum separation conditions for capillary electrophoresesFor all its advantages, capillary electrophoresis (CE) also carries significant disadvantages for the researcher. Offering a unique blend of information from authors active in a variety of developments of chemometrics in CE, Chemometric Methods in Capillary Electrophoresis presents modern chemometric methods as an alternative to help alleviate the problems commonly encountered during routine analysis and method development.Focusing on current chemometric methods utilized in CE endeavours by research-active experts in the field, the book begins with a thorough introduction to CE and chemometric-related concepts and the need for modern chemometric methods in CE.Part 1 discusses differing types of screening designs and response surface methodology)in an)application based formatPart 2 includes vital discussion on various exploratory data analysis, prediction, and classification techniques utilized in CE-related studiesPart 3 provides practical information on modelling quantitative structure relationshipsPart 4 explores transformation techniques, in particular fundamental studies and applications of cross-correlation and Hadamard Transform ElectrophoresisShowing how chemometric methods are applied in a wide array of applications including biological, medical, pharmaceutical, food, forensic, and environmental science, Chemometric Methods in Capillary Electrophoresis is not only highly significant to capillary electrophoresis-based endeavours, but instructive for investigators active in other areas of separation science who could benefit from its informative content.

Table of Contents

Preface
Acknowledgements
Editor Biographies
Contributor Affiliations
Glossary of Key Acronyms
Introduction
Capillary Electrophoresis: an Overview
Chemometric Methods and their Importance in Capillary Electrophoresis
Current and Future Application Areas
References
Experimental Design And Optimization Considerations
Experimental Design in Method Optimization and Robustness Testing
Introduction
Aims/Objectives
Optimization
Robustness Testing
Factors and their Levels
Types of Experimental Designs
Responses
Planning and Execution of Experimental Set-up
Data Handling
Summary and Conclusions
Acknowledgments
References
Chemometrical Experimental Design-Based Optimization Studies in Capillary Electrophoresis Applications
Abstract
Introduction
Results and Discussion
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Conclusions
Acknowledgements
References
Application of Chemometric Methods in Drug Purity Determination by Capillary Electrophoresis
Introduction
Experimental Design in Method Development
Applications of Chemometric Methods in Drug Purity Determination
Conclusions and Outlook
References
Optimization of Micellar Electrokinetic Chromatography Separation Conditions by Chemometric Methods
Micellar Electrokinetic Chromatography
Applying Chemometrics to MEKC
Concluding Remarks
References
Chemometric Methods for the Optimization of CE and CE-MS in Pharmaceutical, Environmental, and Food Analysis
Introduction
Pharmaceutical Applications
Environmental Applications
Food Analysis Applications
Related Applications
Concluding Remarks and Future Considerations
Acknowledgements
References
Optimization of the Separation of Amino Acids by Capillary Electrophoresis using Artificial Neural Networks
Introduction
Experimental
Results and Discussion
Conclusion
Acknowledgments
References
Exploratory Data Analysis, Prediction, And Classification
Development of Capillary Electrophoresis Fingerprints and Multivariate Statistics for the Differentiation of Opium and Poppy Straw Samples
Introduction
Experimental
Results and Discussion
Conclusion
Acknowledgements
References
Multivariate Curve Resolution Based on Alternating Least Squares in Capillary Electrophoresis
Introduction
Mathematical Background
Application of Curve Resolution to CE Data
Conclusions
References
Application of Chemometrics in Capillary Electrophoresis Analysis of Herbal Medicines
Introduction
Terms and Procedures for Multivariate Design
Optimization of Sample Preparation using Chemometric Approaches
Optimization of Separation Conditions using Chemometric Approaches
Data Processing using Chemometric Approaches
Conclusion
Acknowledgments
References
Clinical Pattern Recognition Analysis Applying Artificial Neural Networks Based on Principal Component Analysis Input Selection
Introduction
Theory
Experimental
Results and Discussion
Concluding Remarks
Acknowledgements
References
Chemometric Methods Applied to Genetic Analyses by Capillary Electrophoresis and Electrophoresis Microchip Technologies
Introduction
Genetic Markers
Chemometric Approaches to Genetic Analysis
Methods in Phylogenetic Research
Applications
Concluding Remarks
Acknowledgement
References
Exploratory Data Analysis and Classification of Capillary Electrophoretic Data
Introduction
Data Pretreatment
Exploratory Data Analysis
Classification
Conclusions
Summary
Acknowledgments
References
Quantitative Structure Relationships
Chemometrical Modeling of Electrophoretic Mobilities in Capillary Electrophoresis
Abstract
General Objectives and Concepts
Peptide Mobility and Peptide Mapping
Prediction of Electrophoretic Mobility of Organic Acids
Acknowledgements
References
Assessment of Solute-Micelle Interactions in Electrokinetic Chromatography Using Quantitative Structure Retention Relationships
Introduction
Building QSRR from MEKC Data
The Philosophy behind QSRR
Conclusions
Acknowledgements
References
Chemometrical Analysis of Cheese Proteolysis Profiles by Capillary Electrophoresis: Prediction of Ripening Times
Introduction
Experimental
Results and Discussion
References
Transformation Techniques
Transformation Techniques for Capillary and Microchip Electrophoresis
Introduction
Cross Correlation and Hadamard Transform
Fourier Transform
Conclusion
References
Index
Table of Contents provided by Publisher. All Rights Reserved.

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